LCMS_010.pdf - 第16页
16 X “3 W “3 tira 2S4W HW uotu : “0 he “MB “NM “em 3H W uwstl mat* HOH »M0 — US2IM 2S)M — ”1U8 iaw 加加 . USX IE MMT — FIT X J NMH — xua — NMS — 5 ，# 111 ioUm a11lbUrT CancJ.ttl 54.0 j 」.oa MI»A UftM EM IllhUr； X" u”.…
15
Unk
nown
-5
Cone
85.6
213
1.00
00
1.30
86
1-00
00
Unk
nown
•3
Cone
628
440
1.00
00
3.92
90
too
00
Unk
nown
-2
Cone.
18.9
305
1.00
00
252
77
1-00
00
Printed
at
2020/5/15
17:59:42
Cone Cone
Cone Cone
-2 -2
-3
-3
_002
—
一
00。
_001
一
002
Cone Cone Cone Cone
93.0
90.6
219.
222.
055
815
5017
4104
1.00
1.00
1.00 1.00
00
00
00 00
410
3.92
9.72
9.11
26
82
12
56
1.00
1.00
1.00 1.00
00
00 00
00
Insight
Report
Rex"
File
•
MPA
MRM
edge
m«hod
i,2DS」ue
Blank
-syst
em
Blank
-solve
nt
Cone-1
一
001
Cone-1
.002
Cone-1
.003
Cone
-2
一
001
#
Name
Cone Cone Cone Cone Cone Cone
1
MPA-gluc
—
— ——
1529
15.57
1535
940
47
02
27
572
2
dJ-MPA
—
1.0000 1.0000 1.0000 1.0000
1.00
-glue
00
3
MPA
....
••••
0.8302
0.9007
0.8956
4.07
15
4
dJ-MPA
—
1.0000 1.0000 1.0000 1.0000
1.00
00
Cone
-3
_003
QC-L1
.001
QC-L1
.002
QC-L2
.001
QC-L2
_002
Unk
novffi
-1
#
Name
Cone. Cone.
Cone Cone Cone
Cone.
1
MPA-gluc
213.6
261
44.72
98
44.12
76
135.9
5S4
1352
186
2
d3-MPA
-glue
1.0000
1.0000 1.0000 1.0000 1.0000
3
MPA
9.3945
i0028
20142
5.7061
5.6586
4
d3-MPA
1.0000
1.0000 1.0000 1.0000 1.0000
00
00
Unkn
own-6
QC-L1
_003
QC-L1
_004
QC-L1
_005
QC-L2
_003
QC
-12
一
004
QC
42
_005
Name
Cone Cone Cone Cone Cone Cone
Cone.
1
MPA-gluc
26.18
44do
43.69
4421
［必
132.
135.
46
85
33
18
136
2459
1445
2
dJ-MPA
1.0000
1.0000 1.0000 1.0000 1.0000
1.00 1.00
*
00 00
3
MPA
2.7208
1.9620
1.8611
15490
工甜药
5B5
01
5.59
01
4
dJ-MPA
1.0000
1.0000 1.0000 1.0000 1.0000
1.00 1.00
ID1:
MPA-gluc
Blank
system
Blank-solvent
Cone-1001
Cone-1002
Cone
—
Cone
—
Cone
1
52947
Cone
1
5.5702
Area
-
---
Area
-
…
Area
495314
Area
492209
Q51420>207.10(+)
3.03e2
Q
51420»
207.1
0
(♦)
192。
Q
51420»
207.1
0
(♦)
227e5
Q
51
420>
207.1
0
(+)
228e5
RT
(min)
RT
(mm)
RT
(min)
RT
(mm)
G\Users\skcsl
l\Desktop\damodata\LCMS\test.
iproc
Pagel
of
10
Flagged
Report
打印
被标志
化合物
的结果
图
Report
Options
X
Data
selection
method:
Highlighted
Samples
Highlighted
Compounds
Checked
Samples
Checked
Compounds
旦
。
良
Comparison
Comparison
Report
打印比
较结果
16
X
“3
W
“3
tira
2S4W
HW
uotu
:
“0
he
“MB
“NM
“em
3H
W
uwstl
mat*
HOH
»M0
—
US2IM
2S)M
—
”1U8
iaw
加加
.
USX
IE
MMT
—
FIT
X
J
NMH
—
xua
—
NMS
—
5
，#
111
ioUm
a11lbUrT
CancJ.ttl
54.0
j
」.oa
MI»A
UftM
EM
IllhUr；
X"
u”.
1m.
1as
J4.0N
UUOtar
MM
MtM
y
QCU.t
0CUJH
M
“卅叫
0^.―
MH
,2
•
—
—
S・・w
4
.111
A3
ocu_B
oeuwx
julou^
M>o»
OGUJM
y
—
••
、<
Insight
R・port
_
…一
_
—
―
ID1:
MFA
glue
DMIVMM
Or
9MlM
MManeme
…
IO
fMtfUr
Am
CM
t$TD5・
ImB
U
S
MXVV11
”«血
J*
n
till
xmma
01
MX
ItaMM
tr
IX
q
xi&mr
一
心
2
，外的
MiViMita
V
OBN
—
>5
M1V1L42«M
M
—
・
m
以
上
d
F
VBM
M1ML4UC1
<
5・i
，
•
—
•
y—
M1WL420T
y・・
NYV1L42MA
Aceuraeyf%]
34
04
8S.S5
3436
10652
10533
102
JO
99.77
101.10
97.10
Accuracyf%]
Cone
152947
155X2
153527
94.0572
93.0055
9O.M15
219.5017
2224104
213
6261
打印已
选化合
物的校
准曲线
Ar-a
Ratio
11H1
1134B
11.076
26.190
26.521
25.431
Area
Rmq
Area
495314
492339
495R
26€
935€
2644950
2727103
67165SB
M5O511
6907660
Area
221
初
216965
220923
232742
233076
24622S
256X7
253335
270964
Samp*
Narre
Conc-1
Conc-1
Conc-1
Conc-2
Conc-2
Conc-2
Conc-3
Conc-3
Conc-3
Sample
Nacre
Conc-1
Conc-1
Conc-1
Conc-2
Conc-2
Conc-2
Conc-3
Conc-3
Conc-3
ID1:MPA-gluc
Curve
Fit
Linear
|
Weighting:
None
|Zero:
Not
Forced
Quantitative
Method:
Internal
Standard
CMUSaS
公
9993牢
y
・5ri725L・C442Xai
Data
Filename
Conc-1
001
Conc-CttE
Conc-1
.(XB
ConcZoOI
ConcZoQZ
Conc-2.CXB
ConcT：001
Conc-3.002
Conc-3.003
0.8-
0
此
04：
必
0Q
1
0.0
02
04
0.6
0.8
Conc.Ratio
(mg/L)
ID2:
d3-MPA-gluc
Curve
Fit
Linear
|
Weighting:
None
|
Zero:
Not
Forced
Quantitative
Method:
Internal
Standard
W
*
EQW^8
QS，7，“3C48
— — —
— —
—
Data
Rlenime
Conc-1
001
Cotk-1.002
Conc-1
OCB
Conc<001
Conc-2.002
Cog・2_OB
Cone
工
001
Conc-3.002
Conc-3"(XB
Verified
by
Data
path
C:\U
s
e
r
s\s
kes
I
l\Des
ktop\damodata
Page
1
of
\LCMS
3
Processing
file
test.iproc
Batch
file
Project
Name
|
Version
3.7.66.0
Date
2020/5/18
Time
1
3:27:23
Insight
Calibration
Report
User
Admin
国
Report
Options
Flagged
Data
selection
method:
口
Highlighted
Samples
口
Checked
Samples
口
Highlighted
Compounds
口
Checked
Compounds
目
G
Calibration
Report
阻
Report
Options
圆
Calibration
Data
selection
method:
Highlighted
Samples
Checked
Samples
0
Highlighted
Compounds
0
Checked
Compounds
息
G
X
8
888
00
8
8
888888
00
88
17
打印积
分参数
Integration
Report
图
Report
Options
X
层
1
Integration
Data
selection
method:
0
Highlighted
Samples
Highlighted
Compounds
旦
Checked
Samples
叼
Checked
Compounds
昌
。
Project
Version
3.7.66O
Insight
Integration
Report
Date
2020/5/18
Time
11:24:41
UserID
Admin
Inte
nifty
nm®
Program
Default
MPA-
glue
d3-MPA-gluc
MPA
d3-MPA
Algorithm
Chromatop*:
Chromatopac
ChroEatopsc
ChroEatopK
Chromatopa:
integration
Integration
Mode
Auto
Area
AjtoArea AjtoArea
Auto
Area
Auto
Area
Max
Pe・k
1
5 5 5
5
W
时
5
a
s
a
8
Stop*
Dnft
T.DBL
Mm
Ar»*/^eQht
0 0 0 0 0
Cateulmed
By
Area Area
Area Area Area
NoiM/Drtft
Cak-
Settings
Calculation
Method
ASIM ASIM ASIM ASIM
ASIM
Reflect
Smoothing
and
Kuehne
Correction
Off Off Off
Off Off
Mode
Specified Specified
Specified Specified
Specrfted
Speeffed
Range
(mins)
1
-2
1
-2
1
-2
1
-2
1
-2
Vicinity
of
each
Peak
(Blocks)
Interval
(mins)
0.1
0.1 0.1
0.1 0.1
X
Width
stH
486t
knebde
Peak
Detected
Off
Off
0H
Off Off
Detection
Limit
CoeW
33 33
33
33 33
Quantrtatg
Um
it
Coe
ff
10 10 10 10 10
Um
th«
h
•中
t
from
the
extrapdted
baseline
forS/N
Dnft(mini)
0-15 0-15 0-15 0-15 0-15
Advanced
Tailing
Off
Off Off Off
Off Off
Me
Area/Mcght
s
rn«de
effectrve
m
Manual
Off Off
Off
Off Off
Mtegrstion
Smoothing
Method
Standard Standard
Standard Standard Standard
Counts
1
1 1 1 1
Width
[
1
1
[ [
Blank-solvent
Ale
Acquired
201军1&专
21847
Acquired
By-
System
Adm
[•^透田
Method
File:
U\babSolgons\OawWycos*ienda:e'<20l272*0S_lCMS"<W0_rfoptimm6Quan：ltat6_:ss：waA_MRM_cd5c
一
E«thod_
12120s
3aia
%lr
C
：\use^Acsii'<OesirtaBM»«odata\LCMSWar*-so»ve*i:.l<d
vak
1
1
“
volume
1
OOOOjI
|
Tray:
1
Y«8
Max
Peat
S
Width
5
Mod*ed
Yes
Max
pmv
S
wa*r
s
Mod*ed
y«s
Ma
Peat
5
Width：
8
MOd*®d
Y«8
Max
seat
S
W&k
S
Path
C:\U5ers\skc5ll\Desktop\damodata\LCMS
Page
1
of
Processing
file
test.iproc
26
Batch
file
Verified
by
5.
附录
5.1
修改软
件模式
双
击电脑
桌面上
Application
Configuration
图标，
输入
【密
码】
“admin”
图标，
进行
登录。
点击
【
Application】
下拉
菜单，
选择
【
LabSolutions
Insight】
修改
“Set
Processing
Mode”
，点击
“OK”