MIL-STD-202H.pdf - 第213页
MI L - S TD - 202 -2 1 5 4. GENERAL REQUI RE M E N T S 4.1. Material s 4.1.1 Solvent solut io n s . T he s ol v ent s o l ut i ons us ed i n t h i s t es t s ha l l c on s i s t of t he f ol l ow i n g (see tab le I for …

MIL-STD-202-215
METHOD 215
RESISTANCE TO SOLVENTS
1. SCOPE
1.1 Purpose. The purpose of this test is as follows:
a. To verify that markings or color coding will not become illegible or discolored on the parts (including printed
wiring boards) when subjected to solvents and processes normally used to clean solder flux, fingerprints,
and other contaminants from printed-wiring and terminal-board assemblies, etc.
b. To verify that component protective coatings and encapsulant materials are not degraded to the point
where electrical or mechanical integrity is disturbed when subjected to solvents and processes normally
used to clean solder flux, fingerprints, and other contaminants from printed wiring and terminal board
assemblies, etc.
1.2 Formulation of solvents. The formulation of solvents is considered typical and representative of the solvents
used in printed wiring assembly processing of electronic components. Processing conditions are representative of
processes used for printed wiring assembly.
1.3 Checks for conflicts. When this test is referenced, care should be exercised to assure that conflicting
requirements, as far as the properties of the specified finishes and markings are concerned, are not invoked.
2. APPLICABLE DOCUMENTS
2.1 Specifications, standards, and handbooks. The following specifications, standards, and handbooks form a part
of this document to the extent specified herein. Unless otherwise specified, the issues of these documents are those
cited in the solicitation or contract.
FEDERAL SPECIFICATIONS
TT-I-735 - Isopropyl Alcohol
DEPARTMENT OF DEFENSE SPECIFICATIONS
MIL-PRF-680 - Degreasing Solvent
(Copies of these documents are available online at http://quicksearch.dla.mil)
3. DEFINTIONS
This section not applicable to this standard.
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MIL-STD-202-215
4. GENERAL REQUIREMENTS
4.1. Materials
4.1.1 Solvent solutions. The solvent solutions used in this test shall consist of the following (see table I for
summary).
a. A mixture consisting of the following:
1. One part by volume of isopropyl alcohol, American Chemical Society (ACS) reagent grade, or isopropyl
alcohol in accordance with TT-I-735, grade A or B, and
2. Three parts by volume of mineral spirits in accordance with MIL-PRF-680, type I, or three parts by volume of
a mixture of 80 percent by volume of kerosene and 20 percent by volume ethylbenzene.
b. This solvent has been deleted. When a suitable replacement solvent has been determined, it will be added as
solution b.
c. A terpene defluxer consisting of a minimum of 90 percent d-limonene and 10 percent surfactant. 1/
d. A mixture consisting of the following:
1. Forty-two parts by volume water, 1 megohm-cm minimum resistivity.
2. One part by volume of propylene glycol monomethyl ether (glycol ether PM, 1-methoxy-2-propanol).
3. One part by volume of monoethanolamine. 2/
4.1.1.1 Solvent solutions, safety aspects. Solvent solutions listed in 4.1.1a through 4.1.1d exhibit some potential
for health and safety hazards. Safety precautions as listed in the appropriate manufacturers material safety data
sheet shall be observed.
4.1.2 Vessel. The vessel for solvent immersion shall be a container made of non-reactive material and of sufficient
size to permit complete immersion of the specimens in the solvent solutions specified in 4.1.1.
4.1.3 Brush. The brush shall be a toothbrush with a handle made of a non-reactive material. The brush shall have
three or four long rows, 1 and 1/8 ±1/8 inch in length, of hard bristles. Each row shall contain eight to twelve tufts, the
free ends of which shall lie substantially in the same plane. The brush shall be used with a single solvent and when
there is any evidence of softening, bending, wear, or loss of bristles, it shall be discarded.
1/ A commonly used terpene defluxer is BIOACT EC-7R. "BIOACT" is a registered Trademark of Petroferm INC;
"EC-7 and EC-7R" are trademarks of Petroferm INC.
2/ Normal safety precaution for handling this solution (e.g., same as those for diluted ammonium hydroxide)
based on O.S.H.A. rules for monoethanolamine.
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MIL-STD-202-215
4.2. Procedure
4.2.1 Groups. The specimens subjected to this test shall be divided into three groups of approximately equal size.
a. The first group shall be exposed to the solution specified in 4.1.1a.
The solution shall be maintained at a temperature of 25°C ±5°C. The specimens shall be completely
immersed for 3 minutes +0.5, -0 minutes in the specified solution contained in the vessel specified in 4.1.2.
Immediately following immersion, each specimen shall be tested as follows: The bristle portion of the brush,
specified in 4.1.3, shall be dipped in the solution until wetted and the specimen shall be brushed with normal
hand pressure (approximately 2 to 3 ounce force applied normal to the surface) for ten strokes on the portion of
the specimen where marking has been applied. The brush stroke shall be directed in a forward direction across
the surface of the specimen being tested. Immediately after brushing, the procedure shall be repeated two more
times, for a total of three immersions, followed by brushing. After completion of the third immersion and
brushing, the specimens shall be air-blown dry. The specimens shall be inspected in accordance with 5.2.1 and
5.2.2 to determine the extent, if any, of deterioration that has occurred.
b. This solvent solution has been deleted.
c. The second group shall be exposed to the solution specified in 4.1.1c.
The solution shall be maintained at a temperature of 25°C ±5°C. The specimens shall be completely
immersed for 3 minutes +0.5, -0 minutes in the specified solution contained in the vessel specified in 4.1.2.
Immediately following immersion, each specimen shall be tested as follows: The bristle portion of the brush,
specified in 4.1.3, shall be dipped in the solution until wetted and the specimen shall be brushed with normal
hand pressure (approximately 2 to 3 ounce force applied normal to the surface) for ten strokes on the portion of
the specimen where marking has been applied. The brush stroke shall be directed in a forward direction across
the surface of the specimen being tested. Immediately after brushing, the procedure shall be repeated two more
times, for a total of three immersions, followed by brushing. After completion of the third immersion and
brushing, the specimens shall be rinsed in approximately 25°C water and all surfaces air-blown dry. The
specimens shall be inspected in accordance with 5.2.1 and 5.1.2 to determine the extent, if any, of deterioration
that has occurred.
d. The third group shall be exposed to the solution specified in 4.1.1d.
The solution shall be maintained at a temperature of 63°C to 70°C. The specimens shall be completely
immersed for 3 minutes +0.5, -0 minutes in the specified solution contained in the vessel specified in 4.1.2.
Immediately following immersion, each specimen shall be tested as follows: The bristle portion of the brush,
specified in 4.1.3, shall be dipped in the solution until wetted and the specimen shall be brushed with normal
hand pressure (approximately 2 to 3 ounce force applied normal to the surface) for ten strokes on the portion of
the specimen where marking has been applied. The brush stroke shall be directed in a forward direction across
the surface of the specimen being tested. Immediately after brushing, the procedure shall be repeated two more
times, for a total of three immersions, followed by brushing. After completion of the third immersion and
brushing, the specimens shall be rinsed in approximately 25°C water and all surfaces air-blown dry. The
specimens shall be inspected in accordance with 5.2.1 and 5.1.2 to determine the extent, if any, of deterioration
that has occurred.
4.2.2 Optional exposure procedure for the third group. The test specimens shall be located on a test surface of
known area which is located 6 ±1 inches (15 ±2.5 centimeters) below a spray nozzle which discharges .16 ±.005 gpm
(0.62 ±0.02 liters per minute) of solution per in
2
(6.5 square centimeters) of surface area at a pressure of 20 ±5 lbs/in
2
(138 ±34 kilopascal). The solvent shall be held at a temperature range of 63°C to 70°C. The specimens shall be
subjected to this spray for a period of 10 minutes. After completion of the spray exposure, the specimens shall be
thoroughly rinsed in water and all surfaces air-blown dry and inspected in accordance with 5.2.1 and 5.1.2 to
determine the extent, if any, of deterioration that has occurred. If this optional procedure is specified, brushing of the
samples in the third group is not required. If a conflict arises from the use of the spray option, the brush method of
4.2.1d shall be used as the referee procedure. The measurements shown in parentheses are not exact equivalents
and are shown for convenience only.
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