IPC-TM-650 EN 2022 试验方法--.pdf - 第120页
IPC-TM-650 The Institute for Int erconnecting and Packaging E lectronic Circuits 2215 S anders Road • Northbrook, IL 60062-6135 Material in this T est M ethods Manual was vol untaril y establis hed by T echni cal Committ…
The Institute for Interconnecting and Packaging Electronic Circuits
2215 Sanders Road • Northbrook, IL 60062-6135
Material in this Test Methods Manual was voluntarily established by Technical Committees of the IPC. This material is advisory only
and its use or adaptation is entirely voluntary. IPC disclaims all liability of any kind as to the use, application, or adaptation of this
material. Users are also wholly responsible for protecting themselves against all claims or liabilities for patent infringement.
Equipment referenced is for the convenience of the user and does not imply endorsement by the IPC.
Page 1 of 1
IPC-TM-650
TEST
METHODS
MANUAL
1
.0
Scope
This
test
method
is
used
for
determining
that
marking
inks
and/or
color
coding
will
not
become
illegible
or
discolored
when
subjected
to
solutions
that
are
normally
used
as
cleaning
agents
for
printed
boards
or
printed
board
assem¬
blies.
2
.0
Applicable
Documents
None
3
.0
Test
Specimens
Test
specimens
may
consist
of
test
coupons
or
production
printed
boards
with
the
appropriate
markings.
The
amount
or
size
of
the
marking
on
the
test
specimen
shall
be
sufficient
enough
to
satisfactorily
perform
the
procedure
of
section
5.
4
.0
Apparatus
or
Material
4.1
Vessel
for
each
solution
used.
4.2
Toothbrush
or
suitable
applicator
for
each
solution
used.
4.3
Optical
Aid
capable
of
a
3X
magnification.
4.4
Solution
A:
Mixture
of
one
part
isopropyl
alcohol
and
three
parts
by
volume
of
mineral
spirits
at
25
±
5
℃.
4.5
Solution
B:
Terpene
defluxer
consisting
of
a
minimum
of
90%
d-limonene
and
1
0%
surfactant
at
25
±
5
℃.
4.6
Solution
C:
Mixture
of
42
parts
by
volume
of
water
(1
megohm
resistivity),
one
part
by
volume
of
propylene
glycol
monmethyl
ether,
and
one
part
by
volume
of
monoethanola¬
mine
at
63
to
70℃.
5
.0
Procedure
5.1
The
following
procedure
shall
be
using
solutions
A,
B,
and
C
individually.
Number
2.3.4
Subject
Chemical
Resistance,
Marking
Paints
and
Inks
Date
Revision
8/97
B
Originating
Task
Group
Rigid
Board
T.M.
Task
Group,
7-1
1d
5.1.2
The
test
specimens
shall
be
removed
from
the
vessel
and
with
a
toothbrush
(wetted
with
solution)
the
specimen
shall
be
brushed
for
a
minimum
of
10
strokes
on
the
area
where
the
marking
is
present.
5.1.3
Steps
5.1.1
and
5.1.2
shall
be
repeated
on
the
test
specimen
two
additional
times.
5.1.4
After
the
third
submersion
and
brushing,
the
test
specimens
shall
be
air
or
blown
dry.
5.1.5
The
test
specimens
shall
be
evaluated
in
accordance
with
5.2.
5.2
Evaluation
After
the
test
has
been
performed,
the
test
specimens
shall
be
examined
for
any
markings
that
are
miss¬
ing
in
whole
or
part,
faded,
smeared,
blurred
or
shifted
to
the
extent
that
they
cannot
be
identified
from
a
distance
of
150
mm
[6.0
in]
or
by
examining
with
a
optical
aid
using
a
magni¬
fication
of
no
more
than
3X
shall
constitute
a
failure.
6
.0
Notes
6.1
If
test
solutions
other
than
those
described
herein
are
to
be
used,
then
the
solutions
should
be
agreed
upon
between
the
vendor
and
customer
prior
to
testing.
6.2
The
three
solutions
being
used
to
perform
this
test
exhibit
some
potential
for
health
and
safety
hazards.
Safety
precautions
shall
be
observed.
6.3
It
is
the
intent
of
this
test
method
to
subject
a
different
set
of
test
samples
to
each
test
solutions.
It
is
at
the
option
of
the
tester
to
subject
the
samples
through
the
test
solutions
consecutively.
If
the
samples
fail
after
consecutive
solutions
the
test
should
be
performed
with
individual
test
solutions.
5.1.1
The
test
specimens
shall
be
submerged
for
a
mini¬
mum
of
3
minutes
(+
.5
minutes/
-
0.0
minutes)
in
a
vessel
containing
the
solution.
IPC-TM-650
The Institute for Interconnecting and Packaging Electronic Circuits
2215 Sanders Road • Northbrook, IL 60062-6135
Material in this Test Methods Manual was voluntarily established by Technical Committees of the IPC. This material is advisory only
and its use or adaptation is entirely voluntary. IPC disclaims all liability of any kind as to the use, application, or adaptation of this
material. Users are also wholly responsible for protecting themselves against all claims or liabilities for patent infringement.
Equipment referenced is for the convenience of the user and does not imply endorsement by the IPC.
Page 1 of 4
IPC-TM-650
TEST
METHODS
MANUAL
1
.0
Scope
This
method
is
designed
to
evaluate
the
resis¬
tance
of
dielectric
materials
to
organic
chemicals
representa¬
tive
of
those
used
in
printed
board
fabrication
and
assembly.
It
is
intended
to
provide
a
distinction
between
materials
of
varying
chemical
resistance
and,
when
applicable,
an
indica¬
tion
of
the
degree
of
cure.
2
.0
Applicable
Documents
Method
2.2.18,
Determination
of
Thickness
of
Laminates
by
Mechanical
Measurement
Weast,
R.C.,
ORC
Handbook
of
Chemistry
and
Physics,
65th
Edition,
E-37,
1984
3
.0
Test
Specimens
3.1
Number
Unless
otherwise
specified,
three
specimens
shall
be
used.
3.2
Size
Unless
otherwise
specified,
specimen
shall
be
50.8
x
50.8
mm
±
0.5
mm
[2.0
x
2.0
±
0.02
in]
by
the
thick¬
ness
of
the
material
(see
5.1
,
Preparation).
Edges
shall
be
smooth,
whether
by
the
cutting
procedure,
or
by
sanding,
or
other
means.
3.3
Location
Specimen
may
be
cut
from
anywhere
in
the
sheet
of
material,
except
no
specimens
shall
be
taken
closer
than
25.4
mm
[1.0
in]
from
any
edge
as
laminated.
4
.0
Apparatus
or
Material
4.1
Analytical
balance
with
a
draft
shield
and
.001
gram
or
better
resolution.
4.2
Air
circulating
oven,
capable
of
1
05
±
2
℃
[221
±
3.6°F].
4.3
Desiccator
capable
of
maintaining
an
atmosphere
of
less
than
30%
relative
humidity
at
23℃
[73°F].
See
6.2.5
4.4
Cutting
apparatus
such
as
diamond
saw,
shear
paper
cutter
or
router.
4.5
Edge
smoothing
apparatus
such
as
400
grit
or
finer
sandpaper.
Number
2.3.4.2
Subject
Chemical
Resistance
of
Laminates,
Prepreg,
and
Coated
Foil
Products,
by
Solvent
Exposure
Date
Revision
12/94
A
Originating
Task
Group
MIL-P-13949
Test
Methods
Task
Group
(7-1
1b)
4.6
One
liter
battery
jar,
with
cover.
4.7
Metal
tongs
or
forceps.
4.8
Metal
rack
(to
support
specimens
vertically).
4.9
Metal
support
(e.g.,
mounting
clip
used
for
microsec¬
tioning).
4.10
Laminating
press
capable
of
the
specified
temperature
and
pressure.
4.1
1
Timer:
1
hour
with
1
second
resolution.
4.12
Timer:
60
seconds,
1
second
resolution.
4.13
Solvent:
Methylene
Chloride,
Reagent
Grade
or
HPLC
Grade.
MC
recovered
by
distillation
back
to
reagent
grade
may
be
used.
HPLC
Grade
shall
be
used
for
referee
pur¬
poses.
4.14
Prepreg
(for
single
sided
laminate
and
coated
foil
test
only).
4.15
Copper
foil,
1
oz./ft2
treated
(for
prepreg
tests
only).
4.16
Ventilation
hood
4.17
Micrometer,
capable
of
measuring
to
within
0.025
mm
[0.001
in]
4.18
Water
bath
at
23
±
0.5℃
[73
±
0.9°F]-
4.19
Thermometer
capable
of
measuring
to
within
0.1
resolution.
4.20
Etching
system
capable
of
metallic
cladding
removal.
5
.0
Procedure
5.1
Sample
Preparation
5.1.1
Single-sided
Laminate
Single-sided
laminate
less
than
0.5
mm
[0.020
in]
shall
be
laminated
together
with
the
clad
surfaces
facing
out.
Two
plies
minimum
of
prepreg
shall
be
used.
The
prepreg
shall
be
of
the
same
basic
resin
type
IPC-TM-650
Number
Subject Date
Revision
Page 2 of 4
2.3.4.2
Chemical
Resistance
of
Laminates,
Prepreg,
and
Coated
Foil
Products,
by
Solvent
Exposure
12/94
A
and
of
a
thickness
when
cured
not
greater
than
0.13
mm
[0.005
in]
total,
using
the
prepreg
manufacturer's
recom¬
mended
press
cycle.
Laminate
over
0.5
mm
[0.020
in]
shall
be
treated
like
double
clad
laminate
without
lamination.
5.1.2
Resin-coated
Foil
Resin-coated
foil
samples
shall
be
laminated
together
using
at
least
two
plies
of
prepreg
between
the
coated
sides
of
the
foil.
The
prepreg
shall
be
of
the
same
basic
resin
type
and
of
a
thickness
when
cured
not
greater
than
0.127
mm
[0.005
in]
total,
using
a
press
cycle
and
any
subsequent
post
cure
which
meets
the
manufactur¬
er^
recommendations
for
both
the
coated
foil
and
prepreg.
(See
6.2.1.
1)
For
qualification
and
referee
tests,
a
0.50
±
0.10
mm
[0.02
in]
composite
core
is
to
be
built.
5.1.3
Laminate
with
Coated
Foil
Surfaces
Single-sided
laminate
shall
be
tested
after
lamination
as
in
5.1
.1
.
Double¬
sided
laminate
with
coated
foil
on
one
side
shall
have
the
foil
etched
from
the
uncoated
side
and
shall
subsequently
be
laminated
as
5.1.1.
Double-sided
laminate
with
coated
foil
on
both
sides
shall
be
tested
as
is.
5.1.4
Prepreg
Prepreg
shall
be
laminated
to
a
thickness
of
0.50
±
0.10
mm
[0.020
in]
using
treated
copper
foil
on
both
sides
and
following
the
prepreg
manufacturer's
recommended
press
and
post
cure
cycle.
(See
6.2.1
.1)
For
prepreg
less
than
0.13
mm
[0.005
in]
thick
when
cured,
at
least
two
plies
shall
be
bonded
to
either
side
of
an
etched
laminate
of
a
thickness
such
that
the
pressed
sample
satisfies
the
required
thickness.
5.1.5
Double-sided
Laminate
Double-sided
laminate
shall
be
submitted
for
testing
as
is.
5.2
Specimen
Preparation
5.2.1
Etching
Samples,
as
specified
in
3.0,
shall
be
etched
in
accordance
with
standard
industry
practices.
For
referee
purposes,
2.3.6,
2.3.7,
2.3.7.
1
,
or
2.3.7.2
shall
be
used.
5.2.2
Cut
the
specimens
to
size
per
3.2.
Cutting
shall
be
performed
using
apparatus
and
in
such
a
manner
that
pre¬
vents
edge
damage.
Edge
smoothing
is
recommended
to
prevent
excessive
absorption.
5.2.3
Markings
Each
specimen
shall
be
identified
by
mark¬
ing
with
a
lead
pencil
or
equivalent
technique
which
is
not
removed
by
the
solvent
and
which
doesn't
affect
the
results.
5.3
Preconditioning
5.3.1
Measure
and
record
nominal
thickness
of
the
test
specimen
using
IPC-TM-650,
Method
2.2.18.
5.3.2
Place
the
etched
specimens
vertically
in
the
metal
rack
and
dry
the
specimens
in
the
oven
for
60
±
5
minutes
at
105℃
[221
°F].
Air
flow
around
each
specimen
must
be
assured.
5.3.3
Remove
the
specimens
from
the
oven
and
immedi¬
ately
place
in
the
desiccator
to
cool
for
60
±
30
minutes.
5.4
Test
Condition
The
test
shall
be
performed
at
stan¬
dard
laboratory
conditions:
23
±
2
℃
[73
±
0.9°F]
and
50
±
5%
R.H.
5.5
Measurement
5.5.1
Fill
the
battery
jar
with
750
ml
of
solvent
and
maintain
the
solvent
temperature
at
23
±
0.5℃
[73
土
0.9°]
using
the
water
bath.
5.5.2
Remove
the
specimens
individually
from
the
desicca¬
tor
and
weigh
to
the
nearest
milligram
on
the
analytical
bal¬
ance.
Samples
must
be
weighed
within
60
seconds
of
removal
from
the
desiccator.
Record
these
weights
as
.
5.5.3
Place
the
rack
into
the
beaker
of
solvent,
start
the
60
minute
timer
and
using
tongs
place
the
specimens
in
the
rack
at
suitable
intervals
(recommend
approximately
2
minutes).
Insure
that
the
specimens
are
completely
immersed.
5.5.4
Place
the
metal
clip
on
the
balance
and
tare
it
out.
5.5.5
After
10
minutes
+15,
-0
seconds,
using
the
tongs
remove
the
first
specimen
from
the
solvent
and
start
the
60
second
timer.
5.5.6
Slowly
wag
the
specimen
in
the
air.
As
soon
as
the
specimen
is
free
of
surface
wetness,
but
no
longer
than
30
seconds,
place
the
specimen
on
the
balance
supporting
it
on
the
metal
clip
such
that
both
surfaces
of
the
specimen
are
exposed
(placing
the
specimen
flat
on
the
balance
pan
is
not
permitted
since
evaporation
from
the
side
next
to
the
pan
will
be
reduced.)