IPC-TM-650 EN 2022 试验方法--.pdf - 第599页

IPC-A-600 IPC-TM-650 T est M ethods Manual Material in this T est M ethods Manual was voluntarily establis hed by T echni cal Committees of the IP C. This material is advisory only and its use or adaptation is entirely v…

100%1 / 824
ASTM-D-257 D-C Resistance or Conductance of Insulating
Materials
IPC-TM-650
The Institute for Interconnecting and Packaging Electronic Circuits
2215 Sanders Road • Northbrook, IL 60062
Material in this Test Methods Manual was voluntarily established by Technical Committees of the IPC. This material is advisory only
and its use or adaptation is entirely voluntary. IPC disclaims all liability of any kind as to the use, application, or adaptation of this
material. Users are also wholly responsible for protecting themselves against all claims or liabilities for patent infringement.
Equipment referenced is for the convenience of the user and does not imply endorsement by the IPC.
Page 1 of 4
IPC-TM-650
TEST
METHODS
MANUAL
1
.0
Scope
This
test
method
is
designed
to
determine
vol¬
ume
resistivity
and
surface
resistivity
of
metallic-clad
or
unclad
laminates
under
conditions
of
specified
humidity
and
tempera¬
ture
and
at
elevated
temperatures.
2
.0
Applicable
Documents
Method
2.3.6,
Etching,
Ammonium
Persulfate
Method,
2.3.7
Etching,
Ferric
Chloride
Method
2.3.
7.1,
Cupric
Chloride
Etching
Method
2.6.3,
Moisture
and
Insulation
Resistance,
Rigid,
Rigid/Flex
and
Flex
Printed
Wiring
Boards
3
.0
Test
Specimens
3.1
Laminate
thickness
of
0.51
mm
[0.020
in]
or
greater.
Three
specimens
of
dimensions
101
.6
土
3.2
mm
x
101
.6
±
3.2
mm
[4.0
±
0.125
in
x
4.0
±
0.125
in]
by
thickness
shall
be
prepared
for
each
test
condition,
unless
otherwise
specified.
3.2
Laminate
thickness
of
less
than
0.51
mm
[0.020
in].
Three
specimens
of
dimensions
50.8
±
1
.6
mm
x
50.8
±
1
.6
mm
[2.0
±
0.062
x
2.0
±
0.062
in]
by
the
thickness
shall
be
prepared
for
each
test
condition,
unless
otherwise
specified.
4
.0
Equipment
Apparatus
4.1
Conditioning
chamber
capable
of
maintaining
35
土
2
℃
[95
±
3.6°F]
and
90
+5,-0%
relative
humidity.
4.2
Conditioning
chamber
capable
of
attaining
the
tempera¬
ture
and
humidity
conditions
specified
in
IPC-TM-650,
Method
2.6.3.
4.3
Air
circulating
oven
capable
of
maintaining
the
specified
test
temperatures
to
within
土
2
℃
[±3.6°F]-
4.4
Resistance
measuring
instrumentation
capable
of
mea¬
suring
to
1012
meg-ohms,
minimum,
with
an
accuracy
of
±
5
percent
at
its
highest
scale
setting.
The
equipment
shall
have
the
capability
of
applying
500
volts
de
to
the
test
specimen.
Number
2.5.17.1
Subject
Volume
and
Surface
Resistivity
of
Dielectric
Materials
Date
Revision
12/94
A
Originating
Task
Group
MIL-P-13949
Test
Methods
Task
Group
(7-1
1b)
4.5
A
system/fixture
for
electrical
connections
into
the
tem¬
perature
and
humidity
chambers
(see
4.1
,
4.2,
4.3).
Three
separate
cables
shall
be
provided
to
make
connections
to
each
specimen
being
conditioned/tested.
The
center
conduc¬
tor
of
each
cable
shall
be
connected
to
one
of
the
three
elec¬
trodes
applied
to
the
test
specimen.
The
opposite
ends
of
the
cables
shall
be
brought
outside
the
chamber
and
terminated
at
a
convenient
location
for
connection
to
the
measuring
instrument.
Shields
shall
be
trimmed
back
from
the
ends
of
the
center
conductor
insulation
and
interconnected
to
the
guard
post
of
the
measuring
instrument.
See
6.2
for
additional
information.
Support
the
specimen
parallel
to
the
air
flow
through
the
chamber
during
conditioning.
Special
care
should
be
taken
to
ensure
that
materials
used
in
the
fixture
are
such
that
resistance
readings
are
that
of
the
material
being
tested
and
not
the
fixture.
4.6
A
measurement
device
capable
of
measuring
laminate
thickness
to
the
nearest
0.0025
mm
[0.0001
in].
4.7
Material
and
apparatus
for
formation
of
specimen
con¬
ductors.
4.7.1
Conductor
silver
paint;
composition
4817
by
Dupont
Company,
or
equivalent.
4.7.2
A
system
for
applying
the
paint
to
the
specimen,
such
as
silk
screening.
4.7.3
A
mask,
fixture,
photoprinting
system,
or
equivalent,
for
applying
the
applicable
electrodes/test
pattern
to
the
specimen
(See
Dimension
Table).
4.8
Etching
system
in
accordance
with
IPC-TM-650,
Method
2.3.6,
2.3.7,
or
2.3.7.1
.
5
.0
Procedure
5・1
Specimen
Preparation
5.1.1
Test
patterns
with
the
applicable
dimensions
shown
in
the
Dimension
Table,
and
in
accordance
with
Figures
1
,
2,
and
3
shall
be
generated,
as
follows:
IPC-A-600
IPC-TM-650 Test Methods Manual
Material in this Test Methods Manual was voluntarily established by Technical Committees of the IPC. This material is advisory only
and its use or adaptation is entirely voluntary. IPC disclaims all liability of any kind as to the use, application, or adaptation of this
material. Users are also wholly responsible for protecting themselves against all claims or liabilities for patent infringement.
Equipment referenced is for the convenience of the user and does not imply endorsement by the IPC.
Page 1 of 2
r
ASSOCIATION
CONNECTING
/
ELECTRONICS
INDUSTRIES
221
5
Sanders
Road
Northbrook,
IL
60062-6135
IPC-TM-650
TEST
METHODS
MANUAL
1
Scope
This
test
method
is
designed
to
determine
the
capability
of
HDI
materials
and
other
dielectrics
to
withstand
moisture
induced
stress
as
applied
by
extended
time
in
a
pressure
vessel.
For
laminated
constructions,
the
results
may
be
affected
by
the
process
conditions.
2
Applicable
Documents
Acceptability
of
Printed
Boards
2
.1.1
Microsectioning
2.1
.1
.2
Microsectioning
—
Semi
or
Automatic
Technique
Microsection
Equipment
(Alternate)
2.3.6
Etching,
Ammonium
Persulfate
Method
2.3.7
Etching,
Ferric
Chloride
Method
2.3.7.
1
Cupric
Chloride
Etching
Method
2.3.
7.
2
Alkaline
Etching
Method
3
Test
Specimen
3.1
Samples
shall
be
prepared
as
appropriate
for
the
type
of
material.
All
samples
shall
be
10
cm
x
10
cm
±
0.5
cm,
with
the
thickness
determined
by
the
type
of
material
(see
3.1.1
to
3.1
.3).
Three
samples
shall
be
prepared.
Control
samples
are
required
for
all
samples
where
the
dielectric
layer
is
applied
to
an
etched
laminate.
One
control
sample
of
the
etched
lami¬
nate
(with
no
added
dielectric)
is
required
for
samples
pre¬
pared
according
to
3.
1.2.
2
or
3.1.3.
3.1.1
Copper-Clad
Laminate
The
laminate
shall
have
all
copper
removed
in
accordance
with
IPC-TM-650,
Method
2.3.6,
2.3.7,
2.3.7.
1
or
2.
3.
7.2,
then
cut
to
dimensions
of
10
cm
x
1
0
cm
±
0.65
cm.
3.1.2
Semi-Cured
Prepreg
The
prepreg
shall
be
lami¬
nated
to
a
cured
sheet
configuration,
with
35
micron
copper
foil,
using
the
supplier's
recommended
lamination
cycle.
The
laminate
shall
be
etched
of
all
copper,
then
cut
to
dimensions
of
1
0
cm
x
1
0
cm
±
0.65
cm.
3.
1.2.1
Semi-Cured
Prepreg
or
Dielectric
Material,
Method
A
Sufficient
plies
of
prepreg
shall
be
used
to
result
in
a
composite
base
thickness
of
0.4
mm
±
0.1
mm.
If
the
prepreg
is
of
a
nature
that
does
not
allow
for
lamination
of
a
Number
2.6.16.1
Subject
Moisture
Resistance
of
High
Density
Interconnection
(HDI)
Materials
Under
High
Temperature
and
Pressure
(Pressure
Vessel)
Date
8/98
Revision
Originating
Task
Group
HDI
Test
Methods
Task
Group
(D-42A)
single
sample
of
the
thickness
specified,
then
a
thinner
sample
shall
be
laminated,
noting
the
thickness
as
part
of
the
report,
see
5.5.
3.
1.2.
2
Semi-Cured
Prepreg
or
Dielectric
Material,
Alternate
Method
B
The
prepreg
or
dielectric
layer
shall
be
laminated
to
both
sides
of
an
etched
laminate
that
has
a
thick¬
ness
of
0.4
mm
土
0.1
mm.
The
prepreg
or
dielectric
layer
shall
be
applied,
laminated
and
cured
according
to
the
manufactur¬
er's
recommendations.
Unless
otherwise
specified,
the
result¬
ing
prepreg
or
dielectric
layer
thickness
shall
be
a
nominal
of
0.05
mm
on
each
side
of
the core
laminate.
Optionally,
the
actual
thickness
may
be
measured
by
mechanical
or
cross-
sectional
methods
and
reported,
see
5.5.
Control
samples
shall
be
the
etched
laminate
core
with
no
prepreg
or
dielectric
layer.
3.1.3
Coated
Dielectrics
The
coated
dielectrics
(i.e.,
res¬
ins,
adhesives,
dry
films)
shall
be
applied
to
both
sides
of
an
etched
laminate
that
has
a
thickness
of
0.4
mm
±
0.1
mm.
The
coated
dielectrics
shall
be
applied
and
cured
according
to
the
manufacturer's
recommendations.
Unless
otherwise
specified,
the
resulting
coated
dielectric
thickness
shall
be
a
nominal
of
0.05
mm
on
each
side
of
the
core
laminate.
Optionally,
the
actual
thickness
may
be
measured
by
mechanical
or
cross-sectional
methods
and
reported,
see
55
Control
samples
shall
be
the
etched
laminate
core
with
no
coated
dielectric.
4
Test
Equipment
4.1
Pressure
vessel
capable
of
maintaining
a
constant
pres¬
sure
of
2
ATM
(14
psig),
and
a
temperature
of
121℃
±
2
℃,
with
water
content
maintained
for
a
minimum
of
six
hours
before
needing
replenishment.
4.2
Oven,
air
circulating,
capable
of
holding
a
temperature
of
105℃
±
2
℃
4.3
Microsectioning
equipment,
including
slug
cutter,
mounting,
grinding,
and
polishing
equipment
(see
IPC-TM-
650,
Method
2.1.1
or
2.
1.1.
2)
4.4
Microscope
capable
of
200X
magnification,
with
optional
photographic
equipment
IPC-TM-650
Page 2 of 2
Number
2.6.16.1
Revision
Subject
Moisture
Resistance
of
High
Density
Interconnection
(HDI)
Materials
Under
High
Temperature
and
Pressure
(Pressure
Vessel)
Date
8/98
5
Procedure
5.1
Prepare
specimens
as
required,
depending
on
the
con¬
figuration
of
the
material
under
test
(see
3.1).
5.2
Preconditioning
The
samples
and
controls
shall
be
dried
by
baking
at
1
05℃
土
2
℃
for
a
minimum
of
two
hours
to
remove
moisture.
5.3
Expose
to
Moisture
Under
Pressure
5.3.1
Place
three
pieces
of
each
type
of
material
to
be
tested
in
the
pressure
vessel,
such
that
they
are
vertical
by
use
of
a
rack
or
grooved
block,
which
does
not
cover
more
than
5%
of
the
surface
area
of
the
specimen.
If
samples
have
been
prepared
as
per
3.
1.2.
2
and
3.1
.3,
place
one
piece
of
the
base
laminate
in
the
vessel
along
with
the
specimens.
5.3.2
Fill
the
pressure
vessel
with
water
such
that
the
speci¬
mens
are
not
sitting
in
the
water.
5.3.3
Close
the
lid
of
the
pressure
vessel
and
seal
the
chamber.
5.3.4
Apply
heat
to
the
pressure
vessel
until
the
temperature
and
pressure
specified
are
attained
and
held
constant.
5.3.5
Water
must
be
replenished
during
the
pressure
vessel
test
to
maintain
the
prescribed
pressure
level.
The
interval
of
replenishment
should
not
be
less
than
six
hours.
5.3.6
After
the
required
time,
which
shall
be
96
hours
unless
otherwise
specified,
remove
the
pressure
cooker
from
the
heat
source
and
open
the
chamber.
Remove
the
specimens
and
lay
on
a
countertop
to
stabilize
at
room
temperature.
5.4
Evaluation
5.4.1
Inspect
the
surface
area
of
the
specimens
using
20/20
vision.
When
applicable,
refer
to
IPC-A-600
to
assess
degra¬
dation,
such
as
measling
or
crazing.
5.4.1.
1
Determine
and
grade
the
presence
of
any
degrada¬
tion
(see
5.5.
1.1
through
5.5.1
.5)
or
other
defects,
such
as
measling,
dryness,
loss
of
surface
resin,
etc.
Use
the
uncon¬
ditioned
specimen
from
each
sample
as
a
control
to
contrast
with
the
conditoned
specimens.
For
samples
prepared
as
per
3.1
.2.2
or
3.1
.3,
use
the
base
laminate
as
control.
5.4.1.
2
Record
any
defects
or
degradation
of
the
material.
Note
the
presence
of
any
defects
in
the
unconditioned
con¬
trol.
Include
the
approximate
number
and
size
of
defects
and
the
total
area
of
the
specimen
surface
that
is
afflicted
with
the
defect(s).
5.4.2
When
required
by
the
procurement
documentation,
microsectioning
shall
be
conducted
as
stated
in
5.421
through
5.4.2.
3.
5.4.2.1
Cross
section
at
least
one
specimen
in
the
center
of
the
specimen
in
accordance
with
Method
2.1
.7.
Mount
a
sec¬
tion
of
the
control
of
that
material
beside
the
conditioned
sec¬
tion.
5.4.2.2
After
polishing
the
sections,
examine
under
100
-
200X.
5.
4.
2.
3
Determine
the
presence
of
voids,
resin-to-
reinforcement
separation,
or
other
defects
in
both
the
control
and
the
conditioned
specimen.
5.5
Report
Report
the
base
thickness
of
the
laminate.
For
prepregs
or
coating
et
al,
if
a
composite
sample
is
fabricated,
include
the
final
thickness
of
the
material
in
question
and
the
thickness
of
the
core
laminate.
5.5.1
Report
the
condition
of
the
specimens
according
to
the
following
grade
system.
If
significant
differences
are
noted
between
specimens
of
one
material,
note
the
worse
condition.
Exclude
the
outer
7
mm.
5.5.1.
1
Grade
5
No
measling,
delamination,
dryness,
void¬
ing
or
other
degradation
in
excess
of
that
observed
on
the
unconditioned
sample.
5.5.1.
2
Grade
4
Very
slight
measling;
or
slight
dryness.
5.5.1.
3
Grade
3
Slight
measling
or
dryness;
or
maximum,
of
three
voids
no
greater
than
0.25
mm.
5.5.1.
4
Grade
2
Moderate
measling
or
dryness;
moderate
dryness;
or
more
than
three
voids
no
greater
than
0.5
mm.
5.5.1.
5
Grade
1
Heavy
measling
and
dryness;
or
voids
greater
than
0.5
mm;
blisters
or
delamination.
5.5.2
Optional
Microsectioning
Evaluation
Report
the
presence
of
defects
in
both
control
and
conditioned
speci¬
mens.