IPC-TM-650 EN 2022 试验方法.pdf - 第395页

4.2 Sample Preparation The required square notch is cut in the center of the sample width, within ± 0.25 mm, using a diamond saw or similar stress-free method to form a smooth bottom of the notch. The slot width should b…

1 Scope This test method establishes a procedure for

characterizing the toughness of the resin system materials

used in making laminates for the fabrication of printed wiring

boards. The single-edge-notch bending (SENB) geometry is

used to determine the critical-stress-intensity factor, K

, and

the energy per unit area of crack surface or critical strain

energy release rate, G

, at fracture initiation. This method

assumes linear elastic behavior of the cracked specimen, so

there are corresponding restrictions on the linearity of the

load-displacement diagram. Use of this test method for

printed wiring board laminate materials or other composites

may not yield comparative results.

2 Applicable Documents

2.1 ASTM Standards

D638

Test Method for Tensile Properties of Plastics

D4000 Classification Systems for Specifying Plastic Materials

D5045 Standard Test Methods for Plane-Strain Fracture

Toughness and Strain Energy Release Rate of Plastic

Materials

E399 Test Method for Linear-Elastic Plane-Strain Fracture

Toughness K

of Metallic Materials

E691 Practice for Conducting an Inter-Laboratory Study to

Determine the Precision of a Test Method

3 Terminology

3.1 Terms and Definitions (reference ASTM E399)

3.1.1 Compact Tension

Specimen geometry consisting of

single-edge notched plate loaded in tension.

3.1.2 Critical Strain Energy Release Rate (G

) Tough-

ness parameter based on energy required to fracture.

3.1.3 Plane-Strain Fracture Toughness (K

) Toughness

parameter indicative of material fracture resistance.

3.1.4 Single-Edge Notched Bend Specimen geometry

consisting of center-notched beam.

3.1.5 Yield Stress The stress at fracture (slope of stress-

strain curve is not required to be zero).

4 Test Samples

4.1 Sample Construction

The preferred finished sample is

a block of pure resin, free of contaminants and fully cured (not

partially cured, not over-cured). Note: DSC may be used to

evaluate a received sample’s degree of cure. TGA may be

used to check for the presence of residual solvents or other

contaminants.

A heated hydraulic press may be required to prepare the

sample. Attachment A is a method for making compression

molded thermoset neat resin castings. Size and occurrence of

voids within the sample should be kept to an absolute

minimum (maximum void dimension 25 µm [0.001 in]; maxi-

mum 5 voids/cc). Specimen block may be ground down to

the desired dimensions, and a mold shall not be used.

Default specimen dimensions should be 3.50 mm ± 0.05 mm

thick, 12.7 mm wide (in general, the nominal width can be

between 2X to 4X the thickness, but should be consistent)

and 55.88 mm long (length should be 4.4 times the width).

However the absolute minimum thickness is 2.5 times the

square of the conditional or trial K

) divided by the yield

stress (σ

) of the material for the temperature and loading rate

of the test.

The above should ensure that the sample is wide enough to

ensure plane strain and sufficiently thick to avoid excessive

plasticity in the ligament. If non-linearity in loading still occurs,

the width can be increased up to 4 times the thickness of the

specimen. Polishing the sample (minimum 600 grit) is recom-

mended to promote yielding in the tensile test, rather than

brittle fracture. Each of the thickness and width dimensions of

the specimen should be measured in at least 3 locations to an

accuracy of 0.1% and both dimensions shall be accurate to

within 1% of nominal. The average of these measurements will

be used in the calculations. At least 10 samples of each mate-

rial are recommended for testing, allowing up to 5 samples for

developing sufficient skill in initiating consistent cracks and

subsequently at least 5 samples meeting Section 4.2 criteria

for acceptable fracture toughness measurements.

3000 Lakeside Drive, Suite 309S

Bannockburn, IL 60015-1249

IPC-TM-650

TEST METHODS MANUAL

Number

2.4.52

Subject

Fracture Toughness of Resin Systems for Base

Materials

Date

07/13

Revision

Originating Task Group

IPC 3-11

Material in this Test Methods Manual was voluntarily established by Technical Committees of IPC. This material is advisory only

and its use or adaptation is entirely voluntary. IPC disclaims all liability of any kind as to the use, application, or adaptation of this

material. Users are also wholly responsible for protecting themselves against all claims or liabilities for patent infringement.

Equipment referenced is for the convenience of the user and does not imply endorsement by IPC.

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4.2 Sample Preparation The required square notch is cut

in the center of the sample width, within ± 0.25 mm, using a

diamond saw or similar stress-free method to form a smooth

bottom of the notch. The slot width should be 0.25 mm

[0.00984 in.].

The crack itself is initiated on each sample with a new 0.23

mm [0.009 in] thick ultra-sharp carbon steel razor blade

(example: http://www.mcmaster.com/#3962a4/=3qpeql). It

is recommended that the blade be refrigerated or cooled in

liquid nitrogen or in dry ice shortly before use. The razor blade

is then carefully tapped using a small weighted hammer with

sufficient force and control for the crack to initiate on the first

or second try. A new, cool or cold razor blade is recom-

mended for reducing the force needed for crack initiation. A

few specimens in every test lot should first be sacrificed for

operator practice at crack initiation, precisely determining the

hammer force needed for that sample lot to avoid only mak-

ing indentations. The depth of the natural crack generated by

tapping shall be a least twice the width of the machined

notch (3X the width of the notch is ideal).

The total depth of the notch plus the depth of the crack shall

be half the thickness of the sample, within ± 5 percent. There-

fore the depth of the square notch should be 45 percent of

the sample width minus 0.75 mm, ± 0.13 mm. The crack

shall be sufficiently sharp to ensure that a minimum value

of toughness is obtained during the subsequent 3-point

bending. The actual depths are measured after fracture within

0.5 % accuracy at three locations; at the center of the crack

front, and at the end of the crack front on each surface of the

specimen. The average of these three measurements, which

should be fairly uniform, shall be used in the calculations.

Cracks or breaks should be resin-resin, not between resin and

filler.

5 Equipment/Apparatus or Material

5.1 Test Machine

5.1.1

The testing machine used shall be a constant dis-

placement rate device; an electromechanical screw-driven

machine, or a closed loop feedback-controlled servo-

hydraulic load frame. The stationary and moving rollers used

for the 3-point loading (typically two under each end, and one

on top in the middle of the specimen block opposite the

crack) shall each be large enough to avoid excessive inden-

tation of the plastic, however the roller diameter should not

exceed the overall thickness of the specimen.

5.2 Displacement Measurement

5.2.1

The displacement measurement using an internal

displacement transducer having sufficient precision shall be

performed using the machines stroke or position transducer.

The fracture test displacement data shall be corrected for

system compliance, loading pin penetration and specimen

compression by performing a calibration of the testing sys-

tems as described in ASTM D-5045.

5.2.2 The displacement measurement using an external dis-

placement transducer having sufficient precision shall be

performed with the transducer located between the top and

bottom plates, and as close as possible to the load point on

the specimen to ensure displacement accuracy.

5.3 Yield Stress

5.3.1

The yield stress, σ

, is determined by the material’s

maximum load in an uniaxial tensile test. Using a constant

stroke rate uniaxial tensile test, the loading time to yield shall

be within ± 20 percent of the actual loading time observed in

the fracture test. A zero slope to the stress-strain curve is not

required. If a tensile test cannot be performed, then use 0.7

times the compressive yield stress as an approximation.

6 Procedure

6.1 Test Preparation

The specimens and all testing shall

be performed at 23 °C ± 3 °C. The actual temperature of the

specimen shall be recorded. The relative humidity should be

between 30 % and 60 % RH, and shall be recorded.

6.2 Displacement Correction Specimen shall be identi-

cal to the specimen prepared for fracture testing, except with-

out the notch or crack in the middle. This specimen shall be

used for single notch bend testing (reference ASTM D5045).

6.3 Testing

6.3.1

The notched specimen that has been pre-cracked is

subjected to loading at a loading rate of 5.0 mm per minute.

6.3.2 The test is performed and the load versus loading

point displacement curve is obtained. In the ideal case, there

is an abrupt drop of load to zero at the instant of crack growth

initiation. If this occurs, then determine the trial K

or K

from

the maximum load. Typically there will be a noticeable devia-

tion from linearity prior to fracture.

IPC-TM-650

Number

2.4.52

Subject

Fracture Toughness of Resin Systems for Base Materials

Date

07/13

Revision

Page2of8

6.3.3 The load corresponding to a 2.5 % apparent incre-

ment of crack extension is established by a specified deviation

from the linear portion of the record. The K

value is calcu-

lated from this load by equations that have been established

on the basis of elastic stress analysis on other specimens suf-

ficiently large to show linear elastic behavior.

6.3.4 After breaking, the interface should appear smooth

and glossy. A layered or hazy surface indicates deformation

as a failure mechanism rather than cracking, and invalidates

the test results. After testing, measure the depth of the crack

from the notch depth at three locations along the width of the

sample. Also measure the depth of the crack from the top of

the sample (at the same three locations).

6.3.5 Determining the load displacement area or G

requires an accurate integration of the load versus loading

point displacement curve, including an accurate displacement

determination using the displacement transducer.

7 Analysis Fracture toughness testing is recommended to

be performed at least twice per year.

7.1 Calculation and Interpretation of Results (reference

ASTM D5045, Section 9).

7.1.1

In order to establish that a valid K

has been deter-

mined, it is first necessary to calculate a conditional result, K

which involves a construction on the test record, and to then

determine whether this result is consistent with the size of the

specimen in accordance with 7.1.6. The procedure is given in

7.1.2 through 7.1.8.

7.1.2 Load the specimen and obtain a P (load) versus u

(displacement) plot (see Figure 7-1).

Draw a best straight line (AB) to determine the initial compli-

ance, C. C is given by the reciprocal of the slope of line (AB).

Draw a second line (AB’) with a compliance 5 % greater than

that of line (AB). If the maximum load that the specimen was

able to sustain, Pmax, falls within lines (AB) and (AB’), use

Pmax to calculate K

. If Pmax falls outside line (AB) and line

(AB’), then use the intersection of line (AB’) and the load curve

as P

. Furthermore, if Pmax/P

<1.1, use P

in the calcula-

tion of K

. However, if Pmax/P

>1.1, the test is invalid.

7.1.3 Calculate K

in accordance with the procedure for

single edge notch bending in 7.1.4. For this calculation, a

value of a, which is the total crack length after both notching

and pre-cracking, but before fracture, is best determined from

the fracture surface after testing. An average value is used,

but the difference between the shortest and longest length

should not exceed 10 %. Take care that it is the original crack

which is being observed, since slow growth can occur prior to

catastrophic fast fracture.

7.1.4 (Reference ASTM D5045, Section A1.4). The general

formula for K

calculation of bend specimens is given in [Ref.

3]. The general principles of the bend-test fixture are illustrated

in Figure 7.2.

2-4-52-7-1.eps

Figure 7-1 Determination of C and P

Notes:

• Compliance (C) = tan

θ =

inverse slope of line AB

• 1.05 C = tan θ

max

IPC-TM-650

Number

2.4.52

Subject

Fracture Toughness of Resin Systems for Base Materials

Date

07/13

Revision

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